Insulation materials are essential in building construction; this study proposed to use one such material called silica aerogel, which is known for its excellent thermal properties, and a UV acrylate resin that has been formulated to mix with the aerogel. In this experiment, existing methods of aerogel insulation are discussed and a novel method is investigated. U- value and R- values were obtained by LHICD (i.e., Laser Heating Infrared Camera Detecting method), and K - values were calculated using an equation for 0%, 22.5% and 45% volume of aerogel. The study suggests that using aerogel and resin coating on windows could help to improve the insulating properties of windows. i.e., low thermal conductivity and high thermal resistivity. The results obtained demonstrate that as we increase the percentage volume of aerogel in window coating, the window’s thermal conductivity decreases, and the thermal resistance increases.